Sodium Hydroxide → HCID 11800280, compound

Participants

Reaction Steps

A mixture of the compound obtained in example 51 (0.26 g, 0.5 mmol), 2N NaOH (2.5 mL) and EtOH (25 mL) was stirred at room temperature for 6 days. The solvent was removed and the residue taken up in EtOAc-H2O. The aqueous phase was acidified and extracted with EtOAc, dried and concentrated to afford the desired product as a white solid (0.1 g, 38%).

Provenance & Evidence