HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 400453Generated: November 3, 2026
Triethylammonium hydroxide → HCID 86686051, compound
https://huagongshe.com/reaction/400453
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylammonium hydroxide | HCID 21903323 | — |
| Reactant | Benzyl 3-acetamido-4-oxopyrrolidine-1-carboxylate | HCID 86686050 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86686051 | HCID 86686051 | 31.9% |
Reaction Steps
8.5 g methoxycarbonylsulfamoyl)triethylammoniumhydroxid was added to 4.7 g benzyl 3-acetamido-4-oxopyrrolidine-1-carboxylate in 180 mL THF. The reaction was stirred 1 h at 65° C. and evaporated. The residue was purified on silica gel (hexane/ethyl acetate:1/1) to give 1.4 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08741892B2 |
|---|
| Source dataset | uspto-grants-2014_06 |
|---|
| ORD ID | ord-560ac167e85d483599e1a10467826ce3 |
|---|
| Source note | uspto-grants-2014_06 |
|---|
