HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilyl iodide → HCID 86686052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilyl iodide | HCID 85247 | — |
| Reactant | HCID 86686051 | HCID 86686051 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86686052 | HCID 86686052 | — |
Reaction Steps
0.6 mL trimethylsilyliodide was added to 400 mg 2-methyl-4,6-dihydro-pyrrolo[3,4-d]oxazole-5-carboxylic acid benzyl ester in 30 mL acetonitrile. The reaction was stirred 4 h at RT. The solvent was removed to give 390 mg of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741892B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-1b77d1574e5142bda58aae07ff9ebcb4 |
| Source note | uspto-grants-2014_06 |