HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86686076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86686078 | HCID 86686078 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86686076 | HCID 86686076 | — |
Reaction Steps
1.89 g 3-methyl-5,6,8,9-tetrahydro-imidazo[1,2-a][1,4]diazepine-7-carboxylic acid tert-butyl ester was stirred in 40 mL 4 mol/L HCl solution in dioxane over night. The mixture was concentrated to give 1.67 g of the desired product. Rt: 0.62 min (method AC), (M+H)+: 152
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741892B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-f883dca4e8a34f468c562b3c16b77f06 |
| Source note | uspto-grants-2014_06 |