HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-iodo-6-phenylpyridin-3-ylcarbamate → (4'-Iodo-3,4,5,6-tetrahydro-2H-[1,2]bipyridinyl-5'-yl)carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-iodo-6-phenylpyridin-3-ylcarbamate | HCID 50999073 | — |
| Reactant | Tert-butyl 6-(piperidin-1-yl)pyridin-3-ylcarbamate | HCID 60026701 | — |
| Product | (4'-Iodo-3,4,5,6-tetrahydro-2H-[1,2]bipyridinyl-5'-yl)carbamic acid tert-butyl ester | HCID 60026779 | — |
Reaction Steps
The title product was prepared from (3,4,5,6-tetrahydro-2H-[1,2′]bipyridinyl-5′-yl)carbamic acid tert-butyl ester in the same manner as described in the preparation of (4-iodo-6-phenylpyridin-3-yl)carbamic acid tert-butyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741897B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-fcbc2bc451174145b9c401df778fc444 |
| Source note | uspto-grants-2014_06 |