HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178426390, compound → HCID 178426648, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178426390 | HCID 178426390 | — |
| Reactant | N'-hydroxy-3H-benzimidazole-5-carboximidamide | HCID 178513241 | — |
| Product | HCID 178426648 | HCID 178426648 | — |
Reaction Steps
The title compound was prepared following the procedure described for Intermediate 1, step 2, but starting from 7-methyl-1H-benzimidazole-5-carbonitrile obtained in step 2 (900 mg; 5.73 mmol) as a beige solid (985 mg, 90%). 1H NMR (DMSO-d6) δ 12.60 (br s, 1H), 9.46 (s, 1H), 8.29-7.57 (m, 3H), 5.76 (s, 2H), 2.51 (m, 3H). LC/MS (Method B): 191.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741923B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-2365965f66614fcfb1e437ef2d50b885 |
| Source note | uspto-grants-2014_06 |