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HRID401155

反应详情

EQUATION

反应方程式

HRID 401155 的结构方程式

REACTANTS

反应物

2
结构：Fc1ccc(Br)c(F)c1
HCID67674

1-Bromo-2,4-difluorobenzene

C6H3BrF2

结构：O=C(Cc1ccccc1)c1ccc(-c2ccccc2)cc1
HCID74817

1-(1,1'-Biphenyl)-4-yl-2-phenylethan-1-one

C20H16O

PRODUCTS

生成物

1
结构：O=C(Cc1ccccc1)c1ccc(F)cc1F
HCID43160003

未命名化合物

收率 19%

PROCEDURE

实验过程

Prepared following the procedure described in Intermediate 14, starting from 1-bromo-2,4-difluorobenzene, where the crude product was purified by column chromatography (PE:EtOAc=50:1) to afford Intermediate 21 (250 mg, yield 19%).

WORKUP

后处理

  1. customPrepared
  2. customwas purified by column chromatography (PE:EtOAc=50:1)