HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → 4-Methoxy-3-(2-methoxy-ethoxy)-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | 4-Hydroxy-3-nitro-5-propoxybenzaldehyde | HCID 57354970 | — |
| Product | 4-Methoxy-3-(2-methoxy-ethoxy)-benzaldehyde | HCID 6484657 | 89% |
Reaction Steps
Followed the procedure described in Step 2 of Intermediate 65 starting from 3-hydroxy-4-methoxybenzaldehyde, isolated 2.4 g, yield 89%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08741915B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-aded3f5c37f24d268f15923990a7fd19 |
| Source note | uspto-grants-2014_06 |