Hydrochloric Acid → HCID 25109468, compound

Participants

Reaction Steps

180 mg (0.4 mmol) of 2-(4-methoxy-benzyl)-7-methyl-6-(4-pyrrolidin-1-yl-cyclohexyloxy)-2H-isoquinolin-1-one were heated with 0.9 g trifluoro acetic acid in a microwave oven at 150° C. After aqueous workup, 58 mg of 7-methyl-6-(4-pyrrolidin-1-yl-cyclohexyloxy)-2H-isoquinolin-1-one were obtained as hydrochloride. Rt=1.07 min (Method B). Detected mass: 327.2 (M+H+).

Provenance & Evidence