Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402725Generated: October 31, 2026

HCID 178469744, compound → HCID 178516488, compound

https://huagongshe.com/reaction/402725

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178469744HCID 178469744—
SolventWaterHCID 962—
SolventDimethylacetamideHCID 31374—
ProductHCID 178516488HCID 1785164889%

Reaction Steps

A solution of the compound (0.10 g, 0.31 mmol) of Example 45 in N,N-dimethylacetamide (3.0 mL) was refluxed for 7 h. Cooled to ambient temperature, the reaction mixture was diluted with water and the precipitate was collected by filtration. The solid was washed with water and diethyl ether then dried to afford the titled compound as solid (0.0070 g, y. 9%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742113B2
Source datasetuspto-grants-2014_06
ORD IDord-fed1b5468f3e4ba8860bce620c58129d
Source noteuspto-grants-2014_06