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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402727Generated: October 31, 2026

HCID 178469525, compound → HCID 178516400, compound

https://huagongshe.com/reaction/402727

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178469525HCID 178469525—
SolventDimethylformamideHCID 6228—
ProductHCID 178516400HCID 17851640012.4%

Reaction Steps

A solution of the compound (0.040 g, 0.10 mmol) of Example 59 in N,N-dimethylformamide (2.0 mL) was refluxed for 8 h. Cooled to ambient temperature, the reaction mixture was purified by preparative HPLC to afford the titled compound as solid (0.0040 g, y. 12%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742113B2
Source datasetuspto-grants-2014_06
ORD IDord-f4d0ffc5ba724dbe999d628574d2fb1c
Source noteuspto-grants-2014_06