Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 402728Generated: October 30, 2026

HCID 178469775, compound → HCID 178456796, compound

https://huagongshe.com/reaction/402728

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178469775HCID 178469775—
SolventWaterHCID 962—
SolventDimethylacetamideHCID 31374—
ProductHCID 178456796HCID 17845679613%

Reaction Steps

A solution of the compound (0.15 g, 0.43 mmol) of Example 56 in N,N-dimethylacetamide (1.5 mL) was refluxed for 12 h. Cooled to ambient temperature, the reaction mixture was diluted with water and the precipitate was collected by filtration. The solid was washed with diethyl ether then dried to afford the titled compound as solid (0.015 g, y. 12%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08742113B2
Source datasetuspto-grants-2014_06
ORD IDord-935fdab9fd1d43ab93d665a57720b965
Source noteuspto-grants-2014_06