HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178438838, compound → HCID 178438836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178438838 | HCID 178438838 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178438836 | HCID 178438836 | 81% |
Reaction Steps
Mixture (6) (2.3 g) was hydrogenated in MeOH (50 mL) using Pd/C (10%, dry, 200 mg) and H2 balloon at 1 atm at room temperature for 2 hr. Pd/C was filtered off through a pad of celite and the mother liquid was concentrated to give Compound 2 as white solid (1.13 g, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08742133B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-21a257f963254106b5971593c6cf9e57 |
| Source note | uspto-grants-2014_06 |