Hydrochloric Acid → HCID 46829926, compound

Participants

Reaction Steps

An amount of 123 mg (0.140 mmol) of the compound from example 28A was introduced in 2 ml of dichloromethane and admixed with 1.4 ml (2.807 mmol) of a 2M solution of hydrogen chloride gas in diethyl ether. After 1 hour of stirring, the precipitated solid was isolated by filtration, washed with dichloromethane and diethyl ether and dried under reduced pressure. This gave 79 mg (75% of theory) of the target compound.

Provenance & Evidence