HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane methanol → HCID 86698483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane methanol | HCID 21226129 | — |
| Reactant | 5-(4-Fluoro-2-methoxy-phenyl)-pyridazin-4-ylamine | HCID 86698484 | — |
| Product | HCID 86698483 | HCID 86698483 | — |
Reaction Steps
The title compound was prepared in analogy to example 1, intermediate a, from 5-(4-fluoro-2-methoxy-phenyl)-pyridazin-4-ylamine and using a gradient of dichloromethane:methanol (100:0 to 90:10) for the chromatographic purification. Brown oil (5%). MS (ESI+): m/z=234.1 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748434B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-1149b2e61e49497fa7ff7f28ecae83d8 |
| Source note | uspto-grants-2014_06 |