HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylacetate heptane → N-methyl-5-o-tolylpyridazin-4-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylacetate heptane | HCID 21899848 | — |
| Reactant | 5-o-Tolyl-pyridazin-4-ylamine | HCID 86698486 | — |
| Product | N-methyl-5-o-tolylpyridazin-4-amine | HCID 86698485 | — |
Reaction Steps
The title compound was prepared in analogy to example 8, intermediate a, from 5-o-tolyl-pyridazin-4-ylamine and using a gradient of n-heptane:ethyl acetate (100:0 to 40:60) for the chromatographic purification. Light yellow solid (71%). MS (EI): m/z=199 ([M]).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748434B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-b300b1dcb67c41b4b5db2a5e547945c4 |
| Source note | uspto-grants-2014_06 |