HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl boronic acid → 5-o-Tolyl-pyridazin-4-ylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | 5-Chloropyridazin-4-amine | HCID 13001063 | — |
| Product | 5-o-Tolyl-pyridazin-4-ylamine | HCID 86698486 | — |
Reaction Steps
The title compound was prepared in analogy to example 1, intermediate b, from 5-chloro-pyridazin-4-ylamine (CAS RN 53180-92-0) and 2-methylphenylboronic acid (CAS RN). Light yellow solid (37%). MS (ESI+): m/z=186.103 ([M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748434B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-49b8742bb2c24677ad608e77e44cdb37 |
| Source note | uspto-grants-2014_06 |