P-Anisidine → HCID 66690149, compound

HRID 403532Notes

Reaction equation

HRID 403532 reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]([NH:11][C:12](=O)[CH:13]([Cl:15])[CH3:14])=[C:6]([CH:10]=1)[C:7]([OH:9])=O.[CH3:17]OC1C=CC(N)=CC=1.[CH3:26][C:27]1[CH:32]=[CH:31][C:30]([NH2:33])=[CH:29][CH:28]=1>>[Cl:15][CH:13]([C:12]1[N:33]([C:30]2[CH:31]=[CH:32][C:27]([CH3:26])=[CH:28][C:29]=2[CH3:17])[C:7](=[O:9])[C:6]2[C:5](=[CH:4][CH:3]=[CH:2][CH:10]=2)[N:11]=1)[CH3:14]

Participants

4

Reactant 3

HCID 7732P-AnisidineHCID 7813p-ToluidineHCID 66690534HCID 66690534, compound

Product 1

HCID 66690149HCID 66690149, compound

Procedure

In a similar manner as described above in Paragraph A, but replacing 2-(2-chloropropionylamino)benzoic acid with 5-bromo-2-(2-chloro-propionylamino)benzoic acid and p-anisidine with 4-methyl-phenylamine, the following compound was prepared:

Workup

  1. customthe following compound was prepared

Sources & evidence

ORD record
ord-b68659f635974cf0a9fabcb5796a0030
Source dataset
uspto-grants-2014_06
Patent number
US08748440B2

Reaction notes

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