HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-t-Butylbenzenesulfonyl chloride → HCID 10152782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-t-Butylbenzenesulfonyl chloride | HCID 139882 | — |
| Reactant | HCID 66689784 | HCID 66689784 | — |
| Product | HCID 10152782 | HCID 10152782 | — |
Reaction Steps
In a similar manner as described above in Paragraph A, 5-methoxy-3-(4-methoxyphenyl)-2-(1-methylaminoethyl)-3H-quinazolin-4-one, as prepared above in Example 5, was condensed with 4-tert-butylbenzenesulfonyl chloride to yield 4-tert-butyl-N-{1-[5-methoxy-3-(4-methoxyphenyl)-4-oxo-3,4-dihydroquinazolin-2-yl]ethyl}-N-methylbenzenesulfonamide; MS (ESI) 536 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748440B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-a0b743b716344cbb8f96d5da299ccbd8 |
| Source note | uspto-grants-2014_06 |