HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-isocyanatopropanoate → HCID 66700079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-isocyanatopropanoate | HCID 2733373 | — |
| Reactant | HCID 57419443 | HCID 57419443 | — |
| Product | HCID 66700079 | HCID 66700079 | 83% |
Reaction Steps
3-tert-Butyl-5-iodo-4-methoxyaniline (305 mg, 1 mmol) and ethyl 3-isocyanatopropionate were reacted in the same manner as Example 15 Part A and purified on an Isco 40 g silica cartridge eluting with ethyl acetate/hexane (0% to 25%) to give the title compound (373 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748443B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-90bed1d348d84f6183d4cf8b57fc2373 |
| Source note | uspto-grants-2014_06 |