HRID403882

反应详情

EQUATION

反应方程式

HRID 403882 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The compound of example 223 (0.150 g, 0.000443 mol) was taken in THF (3 mL) and 2-fluorophenyl isothiocyanate (0.074 g, 0.000448 mol) was added and stirred at room temperature for 8-10 h. The reaction mixture was concentrated and directly used for preparation of compound of example 257.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated
  2. customdirectly used for preparation of compound of example 257