HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67360452, compound → HCID 58380189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67360452 | HCID 67360452 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58380189 | HCID 58380189 | — |
Reaction Steps
Compound H6.7 (200 mg, 618 μmol) was dissolved in 5 mL EtOH. To this solution was added palladium on carbon (65.8 mg, 618 μmol) and hydrogen was introduced by balloon. The reaction was stirred at room temperature for 1 hour. After the reaction was complete, the catalyst was filtered off and the solvent was removed to provide H6.8 (135 mg, 93.6%). MS ESI (pos.) m/e: 234.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748462B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-5c7d2b64a4e4483a84f5eab0ffd5272c |
| Source note | uspto-grants-2014_06 |