反应详情

To a stirred solution of T13.2 (530 mg, 1851 μmol) in DCM (15 mL) at 23° C. was added thionyl chloride (270 μL, 3702 μmol). The resulting mixture was stirred overnight and was then concentrated and then purified by silica gel chromatography (0 to 10% EtOAc/hexanes) to provide T13.

1. concentrationwas then concentrated
2. custompurified by silica gel chromatography (0 to 10% EtOAc/hexanes)
3. customto provide T13