HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 58379746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 58380155 | HCID 58380155 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58379746 | HCID 58379746 | — |
Reaction Steps
To a stirred solution of T13.2 (530 mg, 1851 μmol) in DCM (15 mL) at 23° C. was added thionyl chloride (270 μL, 3702 μmol). The resulting mixture was stirred overnight and was then concentrated and then purified by silica gel chromatography (0 to 10% EtOAc/hexanes) to provide T13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748462B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-f4b2619fa6ba4104b07775d78976dae3 |
| Source note | uspto-grants-2014_06 |