HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 58379844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 58380014 | HCID 58380014 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58379844 | HCID 58379844 | — |
Reaction Steps
To a solution of 21.8 (40 mg, 128 μmol) in DCM (0.8 mL), was added thionyl chloride (30 mg, 256 μmol). The resulting mixture was stirred at room temperature for 1 hour. Solvent was removed in vacuo to give a residue which was used without purification (40 mg, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08748462B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-937590881dbc40a89b33a19e492af719 |
| Source note | uspto-grants-2014_06 |