Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrogen Bromide | HCID 260 | — |
| Edukt | (S)-1-(4-Methoxyphenyl)ethylamine | HCID 793467 | — |
| Produkt | HCID 49758827 | HCID 49758827 | — |
Reaktionsschritte
To 11.0 g (72.7 mmol) (S)-1-(4-methoxy-phenyl)-ethylamine is added carefully 30 mL HBr (30% in HOAc). The mixture is stirred at 100° C. for 4 h. After cooling down to r.t., the solvent is removed in vacuo and the residue is dried in vacuo. The resulting product is used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08530460B2 |
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| Quelldatensatz | uspto-grants-2013_09 |
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| ORD ID | ord-388579f90eae45a381a7f25c01287e36 |
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| Quellennotiz | uspto-grants-2013_09 |
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