反应详情

温度

100 °C

To 11.0 g (72.7 mmol) (S)-1-(4-methoxy-phenyl)-ethylamine is added carefully 30 mL HBr (30% in HOAc). The mixture is stirred at 100° C. for 4 h. After cooling down to r.t., the solvent is removed in vacuo and the residue is dried in vacuo. The resulting product is used without further purification.

1. temperatureAfter cooling down to r.t.
2. customthe solvent is removed in vacuo
3. customthe residue is dried in vacuo
4. customThe resulting product is used without further purification