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HRID405931

反应详情

EQUATION

反应方程式

HRID 405931 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：CC(C)(C)OC(=O)N1CCC(CN)(c2ccccc2)CC1
HCID10565452

tert-butyl 4-(aminomethyl)-4-phenylpiperidine-1-carboxylate

C17H26N2O2

PRODUCTS

生成物

1
结构：CC(=O)NCC1(c2ccccc2)CCN(C(=O)OC(C)(C)C)CC1
HCID58117727

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

8 g tert-butyl 4-aminomethyl-4-phenylpiperidine-1-carboxylate and 2.9 ml acetic anhydride are stirred in 80 ml of ethanol overnight at ambient temperature and then evaporated to dryness. 10.4 g product are obtained.

WORKUP

后处理

  1. customevaporated to dryness