HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 405949Generated: October 29, 2026
2-Chlorocyclohexanone → HCID 58080363, compound
https://huagongshe.com/reaction/405949
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Chlorocyclohexanone | HCID 13203 | — |
| Reactant | 1-Benzylpiperidine-4-carboxamide | HCID 783156 | — |
| Product | HCID 58080363 | HCID 58080363 | 70.9% |
Reaction Steps
A mixture of 2.43 g 2-chlorocyclohexanone and 1 g 1-benzylpiperidine-4-carboxylic acid amide (see WO2005/61483) is heated to 160° C. in the microwave until there is no further reaction. The product is purified by chromatography. 963 mg of the product are obtained. Analytical HPLC-MS (method B): RT=1.28 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08754073B2 |
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| Source dataset | uspto-grants-2014_06 |
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| ORD ID | ord-73e7b1ec42b9406591b076b0e4066ea6 |
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| Source note | uspto-grants-2014_06 |
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