HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 58421737, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Reactant | HCID 58421658 | HCID 58421658 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58421737 | HCID 58421737 | — |
Reaction Steps
To (R,R)-4-fluoro-2-(2-hydroxycyclohexyloxy)-nitrobenzene (0.200 g) dissolved in methylene chloride (10.0 ml) was added trimethyloxonium tetrafluoroborate (0.348 g). The mixture was stirred overnight at rt. Water was added; the organic phase was separated and evaporated to dryness to yield a brownish oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754079B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-0d45a76fa01740f6964b6bf8a00ae1e0 |
| Source note | uspto-grants-2014_06 |