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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 406023Generated: October 30, 2026

HCID 58421658, compound → HCID 58421525, compound

https://huagongshe.com/reaction/406023

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58421658HCID 58421658—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 58421525HCID 58421525—

Reaction Steps

(R,R)-4-Fluoro-2-(2-hydroxycyclohexyloxy)-nitrobenzene (1.99 g) in methanol (20.0 ml) was hydrogenated under 50 psi hydrogen for 5 h at rt using palladium on charcoal (5%) (200 mg) as catalyst. The catalyst was filtered off; the resulting solution was evaporated to dryness to yield an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08754079B2
Source datasetuspto-grants-2014_06
ORD IDord-73a3a7e12e3f4ce19c79fca9d88584d2
Source noteuspto-grants-2014_06