HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 66666096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 66665337 | HCID 66665337 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66666096 | HCID 66666096 | — |
Reaction Steps
Ethyl 2-(34(2,3-diphenyl-7,8-dihydropyrido[3,2-b]pyrazin-5(6H)-yl)methyl)phenoxy)acetate (step 2) (163 mg, 0.340 mmol) in EtOH (2 ml) was treated dropwise with 2M NaOH (0.340 ml, 0.680 mmol). The solution was stirred at room temperature for 1 h. The resulting white suspension was collected by filtration, washed with water and dried in a vacuum oven at 40° C. to afford the title compound;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754085B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-dd380506105b4fc0a5bd25f4ce041e99 |
| Source note | uspto-grants-2014_06 |