HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 58351061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | N-(6-bromo-2-methoxypyridin-3-yl)formamide | HCID 71492501 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58351061 | HCID 58351061 | — |
Reaction Steps
Chloroacetone (82 mL) was added dropwise to a suspension of N-(6-bromo-2-methoxypyridin-3-yl)formamide (159.3 g), cesium carbonate (359 g) and potassium iodide (11.4 g) in N,N-dimethylformamide (800 mL) over seven minutes. Then, the reaction solution was stirred at room temperature for one hour and 20 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754100B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-c45e7ddb8c2641b0975c3343edd89d1f |
| Source note | uspto-grants-2014_06 |