HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1-Benzyl-1-methyl-4-oxopiperidinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-Benzyl-4-piperidone | HCID 19220 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Benzyl-1-methyl-4-oxopiperidinium iodide | HCID 11078064 | — |
Reaction Steps
Iodomethane (20.2 ml) was added to a solution of 1-benzyl-4-piperidone (50 ml) in acetone (300 ml) and the mixture was stirred at room temperature overnight. The deposited crystals were collected and washed with acetone to obtain a title compound (77.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754100B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-82209429d3b645338d2f863ffa990e06 |
| Source note | uspto-grants-2014_06 |