HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-1-methylpyridin-2(1H)-one → HCID 59635704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-1-methylpyridin-2(1H)-one | HCID 13024027 | — |
| Reactant | HCID 58109551 | HCID 58109551 | — |
| Product | HCID 59635704 | HCID 59635704 | — |
Reaction Steps
The title compound was prepared from (R)-6-(methoxymethyl)-6-phenyl-3-((S)-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethyl)-1,3-oxazinan-2-one and 5-bromo-1-methylpyridin-2(1H)-one following a procedure analogous to that described in Example 76. Mass spectrum (ESI+): m/z=433 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754076B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-407551e38a4a4cfabfd3dc8c0e44a3e6 |
| Source note | uspto-grants-2014_06 |