HRID407277

反应详情

EQUATION

反应方程式

HRID 407277 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1-(3-Chloropropyl)pyrrolidine (1.142 g) was dissolved in methanol (38 ml) and the solution refluxed overnight. The solution was evaporated to dryness on a rotary evaporator to give 4-azoniaspiro[3,4]octane chloride as an impure oil.

WORKUP

后处理

  1. temperaturethe solution refluxed overnight
  2. customThe solution was evaporated to dryness on a rotary evaporator