HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 178522646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 178509260 | HCID 178509260 | — |
| Product | HCID 178522646 | HCID 178522646 | 90% |
Reaction Steps
A solution of 4-benzothiazol-2-yl-1H-pyrazol-3-ylamine (1.1 g, 5.0 mmol) in 20 mL of formic acid was heated to 70° C. overnight. The formic acid was evaporated under reduced pressure and the resulting crude material was recrystallized from ethanol to yield 1.1 g (90%) of N-(4-benzothiazol-2-yl-1H-pyrazol-3-yl)-formamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08754233B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-95301b1e407147a2b57870a25eb56f71 |
| Source note | uspto-grants-2014_06 |