Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | (11-Bromoundecyl)trichlorosilane | HCID 15895053 | — |
| Solvent | Hexadecane | HCID 11006 | — |
| Product | 11-Bromoundecylsilane | HCID 57350085 | — |
Reaction Steps
Freshly cleaned slides were immersed in a solution of bromoundecyl-trichlorosilane (3% v/v) in hexadecane or toluene. The reaction was heated to 60° C. for 4-6 hours then allowed to cool to room temperature. The slides were washed with CH2Cl2 and ethanol then blown dry under a stream of argon, producing a film with an advancing water contact angle of 82±2 degrees above horizontal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08759008B2 |
|---|
| Source dataset | uspto-grants-2014_06 |
|---|
| ORD ID | ord-7d1aa318407a44748ba2e762b5c1f179 |
|---|
| Source note | uspto-grants-2014_06 |
|---|
