HRID408116

反应详情

EQUATION

反应方程式

HRID 408116 的结构方程式

PROCEDURE

实验过程

A solution of 2-chloro-6-(2-chloro-6-nitrophenylthio)aniline (689 mg, 2.18 mmol) in formic acid (5 mL) was heated at reflux for 16 hours. The mixture was allowed to cool to room temperature and the solvent was evaporated. The residue was used without purification.

WORKUP

后处理

  1. temperatureat reflux for 16 hours
  2. customthe solvent was evaporated
  3. customThe residue was used without purification