HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → N-(2-Chloro-6-(2-chloro-6-nitrophenylthio)phenyl) formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | 2-Chloro-6-(2-chloro-6-nitrophenylthio)aniline | HCID 68227143 | — |
| Product | N-(2-Chloro-6-(2-chloro-6-nitrophenylthio)phenyl) formamide | HCID 86670894 | — |
Reaction Steps
A solution of 2-chloro-6-(2-chloro-6-nitrophenylthio)aniline (689 mg, 2.18 mmol) in formic acid (5 mL) was heated at reflux for 16 hours. The mixture was allowed to cool to room temperature and the solvent was evaporated. The residue was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759336B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-109483b018414b45bc19ae2b0726448b |
| Source note | uspto-grants-2014_06 |