HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25115641, compound → HCID 68725752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25115641 | HCID 25115641 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68725752 | HCID 68725752 | — |
Reaction Steps
6-Benzyloxy-2-methyl-4-(3-phenylpyrrolidin-1-yl)quinoline (0.3 g; see Example 2 above) and palladium on carbon (10%; 0.2 g) in ethanol (8 mL) was stirred under hydrogen for 3 hours. The mixture was filtered and then concentrated to give the title compound as a yellow oil, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759348B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-b6db66f52fb9475c974a9d897396be52 |
| Source note | uspto-grants-2014_06 |