Hydrochloric Acid → HCID 67435180, compound

Participants

Reaction Steps

Add HCl (2.0 M solution in ether) (0.023 g, 0.0006 mol) to a solution of methyl 4-[8-(2-chlorophenyl)-9-(2-hydroxy-2-methyl-propyl)-2-methyl-purin-6-yl]piperazine-1-carboxylate (0.3 g, 0.0006 mol) in ether (4 mL) at 0° C. and stir for 2 h at room temperature. Filter the precipitate, wash with ether, and dry under vacuum to give the title compound (0.24 g) as a white solid. ES/MS m/z 459 (M+1).

Provenance & Evidence