3,4-Dihydro-2-oxo-1(2H)-quinolineacetaldehyde → HCID 24802828, compound

Participants

Reaction Steps

Compound 115 was prepared by the same method as Compound 86 with the exception that Compound 2-3 was used instead of Compound 1-9 and that Compound 1-8 was used instead of Compound 1-4. Compound 115 was isolated as a white solid (53%, mp 243-245° C.). 1H (300 MHz, CDCl3,) δ 7.44-7.01 (m, 8H), 4.55 (m, 2H), 3.62 (m, 2H), 3.31-2.40 (m, 18H); MS (ES+) m/z 440.0 (M+1).

Provenance & Evidence