HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59662176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 59662171 | HCID 59662171 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 59662176 | HCID 59662176 | — |
Reaction Steps
Compound 4-4 (40 mg, 0.11 mmol), dioxane (3 mL), 4N HCl in dioxane (3 mL) and a drop of anisole were added and stirred at rt for 2 hrs. The reaction mixture was concentrated, triturated with ether and dried in vacuo. Compound 4-5 was isolated as a white solid (33 mg, 100%). MS (ES+) m/z 253.7 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759342B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-1e7f5af3e8e0409cbf6f683754b054ce |
| Source note | uspto-grants-2014_06 |