HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 66895060, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 1,2,3,4-Tetrahydro-1-naphthylamine | HCID 18066 | — |
| Reactant | HCID 19358683 | HCID 19358683 | — |
| Product | HCID 66895060 | HCID 66895060 | 70% |
Reaction Steps
0.57 g of tetrahydroquinolino aldehyde was dissolved in 10 ml of methanol and then 0.51 ml of 1,2,3,4-tetrahydro naphthyl amine was slowly added thereto. The resulting mixture was stirred at room temperature overnight before some precipitates were slowly formed. Then, the resulting mixture was filtered while being washed with methanol to provide ivory solids as a clean product (0.72 g). (Yield: 70%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759461B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-94e31b54b11b4b00a907007907c45b94 |
| Source note | uspto-grants-2014_06 |