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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 409612Generated: October 30, 2026

Methanol → HCID 66895060, compound

https://huagongshe.com/reaction/409612

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
Reactant1,2,3,4-Tetrahydro-1-naphthylamineHCID 18066—
ReactantHCID 19358683HCID 19358683—
ProductHCID 66895060HCID 6689506070%

Reaction Steps

0.57 g of tetrahydroquinolino aldehyde was dissolved in 10 ml of methanol and then 0.51 ml of 1,2,3,4-tetrahydro naphthyl amine was slowly added thereto. The resulting mixture was stirred at room temperature overnight before some precipitates were slowly formed. Then, the resulting mixture was filtered while being washed with methanol to provide ivory solids as a clean product (0.72 g). (Yield: 70%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08759461B2
Source datasetuspto-grants-2014_06
ORD IDord-94e31b54b11b4b00a907007907c45b94
Source noteuspto-grants-2014_06