HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18670584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86686116 | HCID 86686116 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18670584 | HCID 18670584 | — |
Reaction Steps
The compound is prepared analogously to Example XI.1 using 4-(4-methoxycarbonylmethyl-phenyl)-piperidine-1-carboxylic acid tert-butyl ester (VIII.2) as educt and TFA in DCM instead of HCl. The crude product is used without further purification in the next reaction step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759528B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-5ba9e19d331845bebe90e4cae54c84cb |
| Source note | uspto-grants-2014_06 |