HRID410352

反应详情

EQUATION

反应方程式

REACTANTS

反应物

反应SMILES：CC(C)(C)OC(=O)NCC(=O)Nc1cccc(Cl)c1

HCID47451221

1,1-Dimethylethyl N-[2-[(3-chlorophenyl)amino]-2-oxoethyl]carbamate

C13H17ClN2O3

PRODUCTS

产物

HCID22690363

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID20443148

1,4-Dioxane hydrochloride

C4H9ClO2

PROCEDURE

实验过程

To [(3-chloro-phenylcarbamoyl)-methyl]-carbamic acid tert-butyl ester (0.7 g, 2.46 mmol) at rt was added 1,4-dioxane HCl (10 ml). The reaction was stirred for 16 h at rt and then filtered. The collected solid was 2-amino-N-(3-chloro-phenyl)-acetamide hydrochloride salt (0.6 g, 100%). HPLC-MS 184, 186 [M+1]+.

WORKUP

后处理

filtrationfiltered