1,1-Dimethylethyl N-[2-[(3-chlorophenyl)amino]-2-oxoethyl]carbamate → HCID 22690363, compound

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Reaction Steps

To [(3-chloro-phenylcarbamoyl)-methyl]-carbamic acid tert-butyl ester (0.7 g, 2.46 mmol) at rt was added 1,4-dioxane HCl (10 ml). The reaction was stirred for 16 h at rt and then filtered. The collected solid was 2-amino-N-(3-chloro-phenyl)-acetamide hydrochloride salt (0.6 g, 100%). HPLC-MS 184, 186 [M+1]+.

Provenance & Evidence