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HRID410717

反应详情

EQUATION

反应方程式

HRID 410717 的结构方程式

REACTANTS

反应物

1
结构：CNC(=O)c1ccc(NC)c([N+](=O)[O-])c1
HCID40234001

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1ccc(NC)c(N)c1
HCID46344445

3-Amino-N-methyl-4-(methylamino)benzamide

C9H13N3O

收率 100.4%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

3-Amino-N-methyl-4-methylamino-benzamide (460 mg) was prepared by following General Procedure B starting from N-methyl-4-methylamino-3-nitro-benzamide (535 mg) and Pd/C (10% by weight, 54 mg). The crude product was used in the next step without further purification.

WORKUP

后处理

  1. customThe crude product was used in the next step without further purification