HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-4-(methylamino)-3-nitrobenzamide → 3-amino-N-methyl-4-(methylamino)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-4-(methylamino)-3-nitrobenzamide | HCID 40234001 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | 3-amino-N-methyl-4-(methylamino)benzamide | HCID 46344445 | 100.4% |
Reaction Steps
3-Amino-N-methyl-4-methylamino-benzamide (460 mg) was prepared by following General Procedure B starting from N-methyl-4-methylamino-3-nitro-benzamide (535 mg) and Pd/C (10% by weight, 54 mg). The crude product was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08759535B2 |
| Source dataset | uspto-grants-2014_06 |
| ORD ID | ord-cb980d97b02f44e09c954a7e21e5ccdb |
| Source note | uspto-grants-2014_06 |